DCPD Cure Kinetics - AC 10/21/22

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Description:

10000:1:1 monomer:G2:TBP or "standard formulation" cure kinetics of "95/5" or 100/5 wt DCPD/ENB

Metadata

Name Value Last Modified
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: DCPD-100ppm_1eqv_10122022
    • Sample Mass (mg): 2.080 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 10/12/2022 5:49:24 PM
    • Operator: ACC
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 326.24
    • Peak temperature (°C): 70.63
    • Onset x (°C): 63.078
    • Max Heat Flow: 6.89
    • Min Baseline Temp: 42.31
    • Max Baseline Temp: 103.198
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Sep 22, 2023
Batch ID
  • Batch ID: 12-10-2022 17:49 AC
  • procedure:
    • Operator Initials: AC
    • Run Date and Time: 2022-10-12 17:49:24
    • Time to DSC (mins after adding catalyst): 5
    • Ambient temperature (°C): 21
    • Relative Humidity (%): null
    • null: null
    • Storage time - postcure (hrs): null
    • Storage Temperature (°C): null
    • Storage condition: null
    • Storage location: null
    • Polymerization method: FROMP
    • Polymerization geometry: Test tube
    • Polymerization Date and Time: 2023-03-29 17:50:00
    • Initiation method: Thermal Soldering
    • Initiation temperature (°C): null
  • inputs:
    • monomers:
        • name: DCPD
        • SMILES: C1C=CC2C1C3CC2C=C3
        • Measured mass (g): null
        • Measured volume (μL): 2843.94
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 2.7870611999999997
        • Molecular Weight: 132.2
        • Moles: 2.11e-02
        • Monomer mol%: 94.79
        • name: ENB
        • SMILES: CC=C1CC2CC1C=C2
        • Measured mass (g): null
        • Measured volume (μL): 156.06
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 0.13936158
        • Molecular Weight: 120.2
        • Moles: 1.16e-03
        • Monomer mol%: 5.21
    • catalysts:
        • name: GC-2
        • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
        • Measured mass (mg): 1.9
        • Computed mass (g): 0.0019
        • Prepared in glovebox?: null
        • Preparation temperature (°C): null
        • Molecular Weight: 848.98
        • Moles: 2.24e-06
        • Monomer:Catalyst molar ratio: 9938.24
    • inhibitors:
        • name: TBP
        • SMILES: CCCCOP(=O)(OCCCC)OCCCC
        • Measured volume (μL): 0.6
        • Prepared in glovebox?: -
        • Preparation temperature (°C): -
        • Density: 0.925
        • Computed mass (mg): 0.0005549999999999999
        • Molecular Weight: 250.3
        • Moles: 2.22e-06
        • Inhibitor:Catalyst molar ratio: 0.99
    • additives:
    • solvents:
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Sep 22, 2023
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: COE_500GC2-curekinetics-12C/min_10122022
    • Sample Mass (mg): 18.380 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 10/12/2022 6:51:23 PM
    • Operator: ACC
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 150.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 198.49
    • Peak temperature (°C): 63.85
    • Onset x (°C): 51.053
    • Max Heat Flow: 23.3
    • Min Baseline Temp: 19.905
    • Max Baseline Temp: 91.473
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Sep 22, 2023
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: DCPD-100ppm_1eqv_10122022
    • Sample Mass (mg): 2.080 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 10/12/2022 5:49:24 PM
    • Operator: ACC
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 326.24
    • Peak temperature (°C): 70.63
    • Onset x (°C): 63.078
    • Max Heat Flow: 6.89
    • Min Baseline Temp: 42.31
    • Max Baseline Temp: 103.198
  • Batch ID: 12-10-2022 17:49 AC
  • procedure:
    • Operator Initials: AC
    • Run Date and Time: 2022-10-12 17:49:24
    • Time to DSC (mins after adding catalyst): 5
    • Ambient temperature (°C): 21
    • Relative Humidity (%): null
    • null: null
    • Storage time - postcure (hrs): null
    • Storage Temperature (°C): null
    • Storage condition: null
    • Storage location: null
    • Polymerization method: FROMP
    • Polymerization geometry: Test tube
    • Polymerization Date and Time: 2023-03-29 17:50:00
    • Initiation method: Thermal Soldering
    • Initiation temperature (°C): null
  • inputs:
    • monomers:
        • name: DCPD
        • SMILES: C1C=CC2C1C3CC2C=C3
        • Measured mass (g): null
        • Measured volume (μL): 2843.94
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 2.7870611999999997
        • Molecular Weight: 132.2
        • Moles: 2.11e-02
        • Monomer mol%: 94.79
        • name: ENB
        • SMILES: CC=C1CC2CC1C=C2
        • Measured mass (g): null
        • Measured volume (μL): 156.06
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 0.13936158
        • Molecular Weight: 120.2
        • Moles: 1.16e-03
        • Monomer mol%: 5.21
    • catalysts:
        • name: GC-2
        • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
        • Measured mass (mg): 1.9
        • Computed mass (g): 0.0019
        • Prepared in glovebox?: null
        • Preparation temperature (°C): null
        • Molecular Weight: 848.98
        • Moles: 2.24e-06
        • Monomer:Catalyst molar ratio: 9938.24
    • inhibitors:
        • name: TBP
        • SMILES: CCCCOP(=O)(OCCCC)OCCCC
        • Measured volume (μL): 0.6
        • Prepared in glovebox?: -
        • Preparation temperature (°C): -
        • Density: 0.925
        • Computed mass (mg): 0.0005549999999999999
        • Molecular Weight: 250.3
        • Moles: 2.22e-06
        • Inhibitor:Catalyst molar ratio: 0.99
    • additives:
    • solvents:
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: COE_500GC2-curekinetics-12C/min_10122022
    • Sample Mass (mg): 18.380 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 10/12/2022 6:51:23 PM
    • Operator: ACC
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 150.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 198.49
    • Peak temperature (°C): 63.85
    • Onset x (°C): 51.053
    • Max Heat Flow: 23.3
    • Min Baseline Temp: 19.905
    • Max Baseline Temp: 91.473
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Fri Sep 22 22:36:55 UTC 2023 PROCESS: Uploading dataset metadata.
Timestamp Status Message
Fri Sep 22 22:17:47 UTC 2023 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Fri Sep 22 22:36:54 UTC 2023 PROCESS: Uploading dataset metadata.

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Last downloaded: Oct 02, 2023 17:29:20
Last Modified: Apr 29, 2025 16:22:14

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