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  2. DCPD:COD 75:25 ...

DCPD:COD 75:25 mol, 4000:1:1 Cure Kinetics ZM-40

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Anna Cramblitt , Zoe Mihevc
Description:

4g DCPD/COD 75/25 mol, 4000:1:1 monomer:G2:TBP, 6.70mg G2, 2.14 uL TBP cure kinetics ZM-40

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Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 17-5-2023 14:36 AC
  • procedure:
    • Operator Initials: AC
    • Run Date and Time: 2023-05-17 14:36:03
    • Time to DSC (mins after adding catalyst): 5
    • Ambient temperature (°C): 21
    • Relative Humidity (%): null
    • null: null
    • Storage time - postcure (hrs): null
    • Storage Temperature (°C): null
    • Storage condition: null
    • Storage location: null
    • Polymerization method: FROMP
    • Polymerization geometry: Test tube
    • Polymerization Date and Time: 2023-05-17 00:00:00
    • Initiation method: Thermal Soldering
    • Initiation temperature (°C): null
  • inputs:
    • monomers:
        • name: DCPD
        • SMILES: C1C=CC2C1C3CC2C=C3
        • Measured mass (g): 3.146
        • Measured volume (μL): null
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 3.146
        • Molecular Weight: 132.2
        • Moles: 2.38e-02
        • Monomer mol%: 75.02
        • name: 1,5 Cyclooctadiene (COD)
        • SMILES: C1/C=C\CC/C=C\C1
        • Measured mass (g): 0.857
        • Measured volume (μL): null
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 0.857
        • Molecular Weight: 108.18
        • Moles: 7.92e-03
        • Monomer mol%: 24.98
    • catalysts:
        • name: GC-2
        • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
        • Measured mass (mg): 6.7
        • Computed mass (g): 0.0067
        • Prepared in glovebox?: No
        • Preparation temperature (°C): RT
        • Molecular Weight: 848.98
        • Moles: 7.89e-06
        • Monomer:Catalyst molar ratio: 4019.26
    • inhibitors:
        • name: TBP
        • SMILES: CCCCOP(=O)(OCCCC)OCCCC
        • Measured volume (μL): 2.144
        • Prepared in glovebox?: -
        • Preparation temperature (°C): -
        • Density: 0.925
        • Computed mass (mg): 0.0019832
        • Molecular Weight: 250.3
        • Moles: 7.92e-06
        • Inhibitor:Catalyst molar ratio: 1.0
    • additives:
    • solvents:
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Oct 31, 2023
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: 1-40_ZM_4000-1-1
    • Sample Mass (mg): 2.760 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 5/17/2023 2:36:03 PM
    • Operator: ACC
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 412.18
    • Peak temperature (°C): 67.17
    • Onset x (°C): 57.42
    • Max Heat Flow: 7.79
    • Min Baseline Temp: 24.279
    • Max Baseline Temp: 136.733
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Oct 31, 2023
  • Batch ID: 17-5-2023 14:36 AC
  • procedure:
    • Operator Initials: AC
    • Run Date and Time: 2023-05-17 14:36:03
    • Time to DSC (mins after adding catalyst): 5
    • Ambient temperature (°C): 21
    • Relative Humidity (%): null
    • null: null
    • Storage time - postcure (hrs): null
    • Storage Temperature (°C): null
    • Storage condition: null
    • Storage location: null
    • Polymerization method: FROMP
    • Polymerization geometry: Test tube
    • Polymerization Date and Time: 2023-05-17 00:00:00
    • Initiation method: Thermal Soldering
    • Initiation temperature (°C): null
  • inputs:
    • monomers:
        • name: DCPD
        • SMILES: C1C=CC2C1C3CC2C=C3
        • Measured mass (g): 3.146
        • Measured volume (μL): null
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 3.146
        • Molecular Weight: 132.2
        • Moles: 2.38e-02
        • Monomer mol%: 75.02
        • name: 1,5 Cyclooctadiene (COD)
        • SMILES: C1/C=C\CC/C=C\C1
        • Measured mass (g): 0.857
        • Measured volume (μL): null
        • Prepared in glovebox?: no
        • Preparation temperature (°C): RT
        • Computed mass (g): 0.857
        • Molecular Weight: 108.18
        • Moles: 7.92e-03
        • Monomer mol%: 24.98
    • catalysts:
        • name: GC-2
        • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
        • Measured mass (mg): 6.7
        • Computed mass (g): 0.0067
        • Prepared in glovebox?: No
        • Preparation temperature (°C): RT
        • Molecular Weight: 848.98
        • Moles: 7.89e-06
        • Monomer:Catalyst molar ratio: 4019.26
    • inhibitors:
        • name: TBP
        • SMILES: CCCCOP(=O)(OCCCC)OCCCC
        • Measured volume (μL): 2.144
        • Prepared in glovebox?: -
        • Preparation temperature (°C): -
        • Density: 0.925
        • Computed mass (mg): 0.0019832
        • Molecular Weight: 250.3
        • Moles: 7.92e-06
        • Inhibitor:Catalyst molar ratio: 1.0
    • additives:
    • solvents:
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: 1-40_ZM_4000-1-1
    • Sample Mass (mg): 2.760 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 5/17/2023 2:36:03 PM
    • Operator: ACC
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 412.18
    • Peak temperature (°C): 67.17
    • Onset x (°C): 57.42
    • Max Heat Flow: 7.79
    • Min Baseline Temp: 24.279
    • Max Baseline Temp: 136.733
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Tue Oct 31 22:19:32 UTC 2023 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Tue Oct 31 22:17:59 UTC 2023 PROCESS: Uploading dataset metadata.

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Last viewed: Jun 14, 2025 14:39:14
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Last Modified: Apr 29, 2025 16:18:55

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