Clowder
  1. Front velocities
  2. 75k_1_2 (1) Pur...

75k_1_2 (1) Pure COD

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Description:

7/17/24

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Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 17-6-2024 13:30 RC
  • procedure:
    • general:
      • Operator Initials: RC
      • Mix Date and Time: 2024-06-17 13:30:00
      • Polymerization Date and Time: 2024-06-17 13:40:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 3
      • Preparation temperature (°C): 20
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): 23
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-2
      • Resin height (mm): 65
      • Diameter (mm): 9.74
      • Thickness (mm): 0.31
      • Tube length (mm): 75
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: RESISTIVE WIRE
      • Heat Source Name: Kanthal A-1 Annealed ROUND Resistance Wire 24GA
      • Heater diameter (mm): 0.5105
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): 5
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: COD
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 3
          • Measured volume (μL): -
          • Computed mass (g): 3
          • Molecular Weight: 108.18
          • Moles: 2.77e-02
          • Monomer mol%: 100.0
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.315
          • Computed mass (g): 0.000315
          • Molecular Weight: 848.98
          • Moles: 3.71e-07
          • Monomer:Catalyst molar ratio: 74741.39
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.201
          • Density: 0.925
          • Computed mass (mg): 0.000185925
          • Molecular Weight: 250.3
          • Moles: 7.43e-07
          • Inhibitor:Catalyst molar ratio: 2.0
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.125609908168247
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jul 25, 2024
  • Batch ID: 17-6-2024 13:30 RC
  • procedure:
    • general:
      • Operator Initials: RC
      • Mix Date and Time: 2024-06-17 13:30:00
      • Polymerization Date and Time: 2024-06-17 13:40:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 3
      • Preparation temperature (°C): 20
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): 23
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-2
      • Resin height (mm): 65
      • Diameter (mm): 9.74
      • Thickness (mm): 0.31
      • Tube length (mm): 75
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: RESISTIVE WIRE
      • Heat Source Name: Kanthal A-1 Annealed ROUND Resistance Wire 24GA
      • Heater diameter (mm): 0.5105
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): 5
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: COD
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 3
          • Measured volume (μL): -
          • Computed mass (g): 3
          • Molecular Weight: 108.18
          • Moles: 2.77e-02
          • Monomer mol%: 100.0
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.315
          • Computed mass (g): 0.000315
          • Molecular Weight: 848.98
          • Moles: 3.71e-07
          • Monomer:Catalyst molar ratio: 74741.39
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.201
          • Density: 0.925
          • Computed mass (mg): 0.000185925
          • Molecular Weight: 250.3
          • Moles: 7.43e-07
          • Inhibitor:Catalyst molar ratio: 2.0
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.125609908168247
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Thu Jul 25 21:51:21 UTC 2024 PROCESS: Uploading dataset metadata.

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Last viewed: Dec 01, 2024 11:42:18
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Last downloaded: Never
Last Modified: Nov 12, 2024 21:39:22

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