973 (codenb)-gc2-linearfront_curekinetics-12.5c

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Description:

Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 08-4-2022 15:05 JP
  • procedure:
    • general:
      • Operator Initials: JP
      • Mix Date and Time: 2022-04-08 15:05:38
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: 1,5 Cyclooctadiene (COD)
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 1.455
          • Measured volume (μL): -
          • Computed mass (g): 1.455
          • Molecular Weight: 108.18
          • Moles: 1.34e-02
          • Monomer mol%: 97.29
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.045
          • Measured volume (μL): null
          • Computed mass (g): 0.045
          • Molecular Weight: 120.2
          • Moles: 3.74e-04
          • Monomer mol%: 2.71
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: Grubbs Catalyst gen-2 (GC2 - M204)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 1.92
          • Computed mass (g): 0.0019199999999999998
          • Molecular Weight: 848.98
          • Moles: 2.26e-06
          • Monomer:Catalyst molar ratio: 6112.74
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.6
          • Density: 0.925
          • Computed mass (mg): 0.0005549999999999999
          • Molecular Weight: 250.3
          • Moles: 2.22e-06
          • Inhibitor:Catalyst molar ratio: 0.98
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jul 26, 2024
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: 97/3 (COD/ENB)-GC2-LinearFront_curekinetics-12.5C
    • Sample Mass (mg): 3.810 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 4/8/2022 3:05:38 PM
    • Operator: JEP
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 12.5
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 180.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 303.57
    • Peak temperature (°C): 61.66
    • Onset x (°C): 53.268
    • Max Heat Flow: 7.58
    • Min Baseline Temp: 20.353
    • Max Baseline Temp: 117.835
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jul 26, 2024
  • Batch ID: 08-4-2022 15:05 JP
  • procedure:
    • general:
      • Operator Initials: JP
      • Mix Date and Time: 2022-04-08 15:05:38
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: 1,5 Cyclooctadiene (COD)
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 1.455
          • Measured volume (μL): -
          • Computed mass (g): 1.455
          • Molecular Weight: 108.18
          • Moles: 1.34e-02
          • Monomer mol%: 97.29
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.045
          • Measured volume (μL): null
          • Computed mass (g): 0.045
          • Molecular Weight: 120.2
          • Moles: 3.74e-04
          • Monomer mol%: 2.71
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: Grubbs Catalyst gen-2 (GC2 - M204)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 1.92
          • Computed mass (g): 0.0019199999999999998
          • Molecular Weight: 848.98
          • Moles: 2.26e-06
          • Monomer:Catalyst molar ratio: 6112.74
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.6
          • Density: 0.925
          • Computed mass (mg): 0.0005549999999999999
          • Molecular Weight: 250.3
          • Moles: 2.22e-06
          • Inhibitor:Catalyst molar ratio: 0.98
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: 97/3 (COD/ENB)-GC2-LinearFront_curekinetics-12.5C
    • Sample Mass (mg): 3.810 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 4/8/2022 3:05:38 PM
    • Operator: JEP
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.0.0.44608
    • Ramp rate (°C/min): 12.5
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 180.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 303.57
    • Peak temperature (°C): 61.66
    • Onset x (°C): 53.268
    • Max Heat Flow: 7.58
    • Min Baseline Temp: 20.353
    • Max Baseline Temp: 117.835
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Fri Jul 26 06:10:08 UTC 2024 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Fri Jul 26 06:10:07 UTC 2024 PROCESS: Uploading dataset metadata.

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Last downloaded: Sep 06, 2024 21:28:20
Last Modified: Apr 29, 2025 16:03:53

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