lerk-iv-109-cod_enb-gc2-240h-s4

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Description:

Metadata

Name Value Last Modified
procedure
  • procedure:
    • Experiment Type: LERK_COD_ENB_POST_CURE
    • Sample Name: LERK-IV-109-COD_ENB-GC2-240h-S4
    • Sample Mass (mg): 5.170 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 2/15/2024 9:06:28 AM
    • Operator: LERK
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 10.0
    • Ramp Min Temp (°C): 20.0
    • Ramp Max Temp (°C): 150.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 67.474
    • Peak temperature (°C): 41.06
    • Onset x (°C): 35.743
    • Max Heat Flow: 0.23
    • Min Baseline Temp: 25.0
    • Max Baseline Temp: 137.339
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jul 31, 2024
Batch ID
  • Batch ID: 05-2-2024 09:06 LERK
  • procedure:
    • general:
      • Operator Initials: LERK
      • Mix Date and Time: 2024-02-05 09:06:28
      • Polymerization Date and Time: 2024-02-05 09:06:28
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): 23.2
      • Polymer Storage armosphere: N2
      • Polymer Storage location: Oven
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): 25
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: MOLD-1
      • Resin Width (mm): 101.6
      • Total width (mm): 90
      • Resin height (mm): 70
      • Total height (mm): 76.2
      • Thickness (mm): 4.2
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: RESISTIVE WIRE
      • Heat Source Name: 24-gauge Kanthal wire
      • Heater diameter (mm): 0.5
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): 6.31
      • Current (A): 3.8
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: COD
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 25.5789
          • Measured volume (μL): -
          • Computed mass (g): 25.5789
          • Molecular Weight: 108.18
          • Moles: 2.36e-01
          • Monomer mol%: 97.25
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.8037
          • Measured volume (μL): null
          • Computed mass (g): 0.8037
          • Molecular Weight: 120.2
          • Moles: 6.69e-03
          • Monomer mol%: 2.75
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 38.4
          • Computed mass (g): 0.0384
          • Molecular Weight: 848.98
          • Moles: 4.52e-05
          • Monomer:Catalyst molar ratio: 5375.41
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 24.9
          • Density: 0.925
          • Computed mass (mg): 0.0230325
          • Molecular Weight: 250.3
          • Moles: 9.20e-05
          • Inhibitor:Catalyst molar ratio: 2.03
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): null
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: SPIN
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jul 31, 2024
  • procedure:
    • Experiment Type: LERK_COD_ENB_POST_CURE
    • Sample Name: LERK-IV-109-COD_ENB-GC2-240h-S4
    • Sample Mass (mg): 5.170 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 2/15/2024 9:06:28 AM
    • Operator: LERK
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 10.0
    • Ramp Min Temp (°C): 20.0
    • Ramp Max Temp (°C): 150.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 67.474
    • Peak temperature (°C): 41.06
    • Onset x (°C): 35.743
    • Max Heat Flow: 0.23
    • Min Baseline Temp: 25.0
    • Max Baseline Temp: 137.339
  • Batch ID: 05-2-2024 09:06 LERK
  • procedure:
    • general:
      • Operator Initials: LERK
      • Mix Date and Time: 2024-02-05 09:06:28
      • Polymerization Date and Time: 2024-02-05 09:06:28
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): 23.2
      • Polymer Storage armosphere: N2
      • Polymer Storage location: Oven
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): 25
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: MOLD-1
      • Resin Width (mm): 101.6
      • Total width (mm): 90
      • Resin height (mm): 70
      • Total height (mm): 76.2
      • Thickness (mm): 4.2
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: RESISTIVE WIRE
      • Heat Source Name: 24-gauge Kanthal wire
      • Heater diameter (mm): 0.5
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): 6.31
      • Current (A): 3.8
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: COD
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 25.5789
          • Measured volume (μL): -
          • Computed mass (g): 25.5789
          • Molecular Weight: 108.18
          • Moles: 2.36e-01
          • Monomer mol%: 97.25
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.8037
          • Measured volume (μL): null
          • Computed mass (g): 0.8037
          • Molecular Weight: 120.2
          • Moles: 6.69e-03
          • Monomer mol%: 2.75
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 38.4
          • Computed mass (g): 0.0384
          • Molecular Weight: 848.98
          • Moles: 4.52e-05
          • Monomer:Catalyst molar ratio: 5375.41
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 24.9
          • Density: 0.925
          • Computed mass (mg): 0.0230325
          • Molecular Weight: 250.3
          • Moles: 9.20e-05
          • Inhibitor:Catalyst molar ratio: 2.03
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): null
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: SPIN
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Wed Jul 31 17:20:34 UTC 2024 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Wed Jul 31 17:20:03 UTC 2024 PROCESS: Uploading dataset metadata.

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Last Modified: Jul 31, 2024 17:20:01

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