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MLI067_4_10242024_P4_2

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Description:

DCPD-DHF, 20 mol% DHF, 1000 ppm GC2, 16 psi N2

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Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 24-10-2024 13:16 MJL
  • procedure:
    • general:
      • Operator Initials: MJL
      • Mix Date and Time: 2024-10-24 13:16:00
      • Polymerization Date and Time: 2024-10-24 13:22:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): 19
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): 20
      • Resin temperaure at the start of polymerization (°C): 19
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-1
      • Resin height (mm): null
      • Diameter (mm): 9.7
      • Thickness (mm): null
      • Tube length (mm): null
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: SODERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: DCPD
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 2.881635
          • Measured volume (μL): null
          • Computed mass (g): 2.881635
          • Molecular Weight: 132.2
          • Moles: 2.18e-02
          • Monomer mol%: 78.91
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.15166500000000002
          • Measured volume (μL): null
          • Computed mass (g): 0.15166500000000002
          • Molecular Weight: 120.2
          • Moles: 1.26e-03
          • Monomer mol%: 4.57
          • name: DHF
          • SMILES: C1COC=C1
          • Measured mass (g): null
          • Measured volume (μL): 345
          • Computed mass (g): 0.319815
          • Molecular Weight: 70.1
          • Moles: 4.56e-03
          • Monomer mol%: 16.52
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 25
        • Mixing type: Sonication
        • Mixing time (mins): 5
    • catalysts:
      • catalyst-inputs:
          • name: GC2, M204
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 23.3
          • Computed mass (g): 0.0233
          • Molecular Weight: 848.98
          • Moles: 2.74e-05
          • Monomer:Catalyst molar ratio: 1006.45
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 25
        • Mixing type: Sonication
        • Mixing time (mins): 5
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.83
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Oct 31, 2024
  • Batch ID: 24-10-2024 13:16 MJL
  • procedure:
    • general:
      • Operator Initials: MJL
      • Mix Date and Time: 2024-10-24 13:16:00
      • Polymerization Date and Time: 2024-10-24 13:22:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): 19
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): 20
      • Resin temperaure at the start of polymerization (°C): 19
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-1
      • Resin height (mm): null
      • Diameter (mm): 9.7
      • Thickness (mm): null
      • Tube length (mm): null
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: SODERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: DCPD
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 2.881635
          • Measured volume (μL): null
          • Computed mass (g): 2.881635
          • Molecular Weight: 132.2
          • Moles: 2.18e-02
          • Monomer mol%: 78.91
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.15166500000000002
          • Measured volume (μL): null
          • Computed mass (g): 0.15166500000000002
          • Molecular Weight: 120.2
          • Moles: 1.26e-03
          • Monomer mol%: 4.57
          • name: DHF
          • SMILES: C1COC=C1
          • Measured mass (g): null
          • Measured volume (μL): 345
          • Computed mass (g): 0.319815
          • Molecular Weight: 70.1
          • Moles: 4.56e-03
          • Monomer mol%: 16.52
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 25
        • Mixing type: Sonication
        • Mixing time (mins): 5
    • catalysts:
      • catalyst-inputs:
          • name: GC2, M204
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 23.3
          • Computed mass (g): 0.0233
          • Molecular Weight: 848.98
          • Moles: 2.74e-05
          • Monomer:Catalyst molar ratio: 1006.45
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 25
        • Mixing type: Sonication
        • Mixing time (mins): 5
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.83
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Thu Oct 31 21:34:10 UTC 2024 PROCESS: Uploading dataset metadata.

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Last viewed: Jul 08, 2025 10:29:12
Downloads: 0
Last downloaded: Never
Last Modified: Oct 31, 2024 21:34:15

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