Clowder
  1. DSC Cure Kinetics
  2. 2 ppm-g3 10 eq-...

2 ppm-g3 10 eq-py 100ppm-psu-g2 92_8-dcpd_enb - ionox ambient - 2024-10-29 - day 150

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Metadata

Name Value Last Modified
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: 2 ppm-G3 10 eq-Py 100ppm-PSU-G2 92_8-DCPD_ENB - IONOX ambient - 2024-10-29 - day 150
    • Sample Mass (mg): 1.840 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 10/29/2024 6:25:54 PM
    • Operator: EL
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.2.101
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 150.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 252.95
    • Peak temperature (°C): 95.05
    • Onset x (°C): 92.848
    • Max Heat Flow: 16.38
    • Min Baseline Temp: 63.912
    • Max Baseline Temp: 142.63
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Nov 4, 2024
Batch ID
  • Batch ID: 01-6-2024 15:10 EL
  • procedure:
    • general:
      • Operator Initials: EL
      • Mix Date and Time: 2024-06-01 15:10:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: Air
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Mechanical
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: null
      • #N/A: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: DCPD
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 285.2
          • Measured volume (μL): null
          • Computed mass (g): 285.2
          • Molecular Weight: 132.2
          • Moles: 2.16e+00
          • Monomer mol%: 91.27
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 24.8
          • Measured volume (μL): null
          • Computed mass (g): 24.8
          • Molecular Weight: 120.2
          • Moles: 2.06e-01
          • Monomer mol%: 8.73
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC2 (polysulfone encapsulated)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 4129.02
          • Computed mass (g): 4.129020000000001
          • Molecular Weight: 848.98
          • Moles: 4.86e-03
          • Monomer:Catalyst molar ratio: 486.0
          • name: GC3
          • SMILES: Brc1cccnc1.Brc2cccnc2.Cc3cc(C)c(N4CCN(C4=[Ru](Cl)(Cl)=Cc5ccccc5)c6c(C)cc(C)cc6C)c(C)c3
          • Measured mass (mg): 30
          • Computed mass (g): 0.03
          • Molecular Weight: 884.54
          • Moles: 3.39e-05
          • Monomer:Catalyst molar ratio: 69691.73
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 64.19
          • Density: 0.925
          • Computed mass (mg): 0.05937575
          • Molecular Weight: 250.3
          • Moles: 2.37e-04
          • Inhibitor:Catalyst molar ratio: 0.05
          • name: Pyridine
          • SMILES: C1=CC=NC=C1
          • Measured volume (μL): 3.83
          • Density: 0.978
          • Computed mass (mg): 0.00374574
          • Molecular Weight: 79.1
          • Moles: 4.74e-05
          • Inhibitor:Catalyst molar ratio: 0.01
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Mechanical
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: 4,4′-Methylenebis(2,6-di-tert-butylphenol)
          • SMILES: CC(C)(C)c1c(C(C)(C)C)c(O)c(C)c(c1)C(C)(C)c2ccccc2C(C)(C)c3c(C(C)(C)C)c(O)c(C)c(c3)C(C)(C)C
          • Measured mass (g): 5.01876
          • Measured volume (μL): null
          • Computed mass (g): 5.01876
          • Molecular Weight: 424.66
          • Moles: 1.18e-02
          • Wt Percent of Additives: 1.57
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Mechanical
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
          • name: Toluene
          • SMILES: CC1=CC=CC=C1
          • Measured mass (mg): null
          • Measured volume (μL): 1146.17
          • Computed mass (mg): 0.9937293900000002
          • Molecular Weight: 92.14
          • Moles: 1.08e-02
          • Solvent concentration: 0.28
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Mechanical
        • Mixing time (mins): null
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Nov 4, 2024
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: 2 ppm-G3 10 eq-Py 100ppm-PSU-G2 92_8-DCPD_ENB - IONOX ambient - 2024-10-29 - day 150
    • Sample Mass (mg): 1.840 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 10/29/2024 6:25:54 PM
    • Operator: EL
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.2.101
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 150.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 252.95
    • Peak temperature (°C): 95.05
    • Onset x (°C): 92.848
    • Max Heat Flow: 16.38
    • Min Baseline Temp: 63.912
    • Max Baseline Temp: 142.63
  • Batch ID: 01-6-2024 15:10 EL
  • procedure:
    • general:
      • Operator Initials: EL
      • Mix Date and Time: 2024-06-01 15:10:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: Air
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Mechanical
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: null
      • #N/A: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: DCPD
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 285.2
          • Measured volume (μL): null
          • Computed mass (g): 285.2
          • Molecular Weight: 132.2
          • Moles: 2.16e+00
          • Monomer mol%: 91.27
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 24.8
          • Measured volume (μL): null
          • Computed mass (g): 24.8
          • Molecular Weight: 120.2
          • Moles: 2.06e-01
          • Monomer mol%: 8.73
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC2 (polysulfone encapsulated)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 4129.02
          • Computed mass (g): 4.129020000000001
          • Molecular Weight: 848.98
          • Moles: 4.86e-03
          • Monomer:Catalyst molar ratio: 486.0
          • name: GC3
          • SMILES: Brc1cccnc1.Brc2cccnc2.Cc3cc(C)c(N4CCN(C4=[Ru](Cl)(Cl)=Cc5ccccc5)c6c(C)cc(C)cc6C)c(C)c3
          • Measured mass (mg): 30
          • Computed mass (g): 0.03
          • Molecular Weight: 884.54
          • Moles: 3.39e-05
          • Monomer:Catalyst molar ratio: 69691.73
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 64.19
          • Density: 0.925
          • Computed mass (mg): 0.05937575
          • Molecular Weight: 250.3
          • Moles: 2.37e-04
          • Inhibitor:Catalyst molar ratio: 0.05
          • name: Pyridine
          • SMILES: C1=CC=NC=C1
          • Measured volume (μL): 3.83
          • Density: 0.978
          • Computed mass (mg): 0.00374574
          • Molecular Weight: 79.1
          • Moles: 4.74e-05
          • Inhibitor:Catalyst molar ratio: 0.01
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Mechanical
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: 4,4′-Methylenebis(2,6-di-tert-butylphenol)
          • SMILES: CC(C)(C)c1c(C(C)(C)C)c(O)c(C)c(c1)C(C)(C)c2ccccc2C(C)(C)c3c(C(C)(C)C)c(O)c(C)c(c3)C(C)(C)C
          • Measured mass (g): 5.01876
          • Measured volume (μL): null
          • Computed mass (g): 5.01876
          • Molecular Weight: 424.66
          • Moles: 1.18e-02
          • Wt Percent of Additives: 1.57
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Mechanical
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
          • name: Toluene
          • SMILES: CC1=CC=CC=C1
          • Measured mass (mg): null
          • Measured volume (μL): 1146.17
          • Computed mass (mg): 0.9937293900000002
          • Molecular Weight: 92.14
          • Moles: 1.08e-02
          • Solvent concentration: 0.28
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Mechanical
        • Mixing time (mins): null
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Mon Nov 04 23:03:22 UTC 2024 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Mon Nov 04 23:03:22 UTC 2024 PROCESS: Uploading dataset metadata.

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