AC-1-252_COD/ENB_1000-1-2-A

Owner: Anna Cramblitt
Created on Nov 15, 2024

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Description:

Monomer:G2:TBP 1000:1:2. 97/3 vol% COD/ENB measured by mass from a large batch. FROMPed at initial resin temperature of 23 degrees C.

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Metadata

Name	Value	Last Modified
Batch ID	Batch ID: 30-10-2024 15:30 ACC procedure: general: Operator Initials: ACC Mix Date and Time: 2024-10-30 15:30:00 Polymerization Date and Time: 2024-10-30 00:00:00 Resin Storage Temperature (°C): null Resin Storage atmosphere: null Resin Storage location: null Polymer Storage Temperature (°C): null Polymer Storage armosphere: null Polymer Storage location: null Mixing Conditions: null Mixing Type: Sonication Mixing Time (min): 2 Preparation temperature (°C): 19 Use Glovebox: NO Polymerization: null Type of polymerization: FROMP Ambient temperature (°C): 21 Resin temperaure at the start of polymerization (°C): 23.1 Select Geometry from geometries tab: null Geometry - Select from library: TUBE-2 Resin height (mm): 65 Diameter (mm): 9.74 Thickness (mm): 0.31 Tube length (mm): 75 Empty-dim: null Initiation: null Initiation method: THERMAL Photocontrol: null Photocontrol?: NO null: null thermal initiation: Heat Source: RESISTIVE WIRE Heat Source Name: Kanthal A-1 Annealed ROUND Resistance Wire 24GA Heater diameter (mm): 0.5105 Submerged length (mm): null Power (W): null Voltage (V): 4 Current (A): 4 Heat source temperature (°C): null Induction time (s): until front starts inputs: monomers: monomer-inputs: name: COD SMILES: C1/C=C\CC/C=C\C1 Measured mass (g): 1.9392744211349495 Measured volume (μL): null Computed mass (g): 1.9392744211349495 Molecular Weight: 108.18 Moles: 1.79e-02 Monomer mol%: 97.26 name: ENB SMILES: CC=C1CC2CC1C=C2 Measured mass (g): 0.06072557886505048 Measured volume (μL): null Computed mass (g): 0.06072557886505048 Molecular Weight: 120.2 Moles: 5.05e-04 Monomer mol%: 2.74 monomer-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): 20 Mixing type: N/A Mixing time (mins): null catalysts: catalyst-inputs: name: GC2, M204 SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3 Measured mass (mg): 15.62 Computed mass (g): 0.015619999999999998 Molecular Weight: 848.98 Moles: 1.84e-05 Monomer:Catalyst molar ratio: 1001.79 catalyst-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): 21 Mixing type: Sonication Mixing time (mins): 2 inhibitors: inhibitor-inputs: name: Tributyl phosphite (TBP) SMILES: CCCCOP(=O)(OCCCC)OCCCC Measured volume (μL): 10 Density: 0.925 Computed mass (mg): 0.009250000000000001 Molecular Weight: 250.3 Moles: 3.70e-05 Inhibitor:Catalyst molar ratio: 2.01 inhibitor-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null additives: additive-inputs: additive-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null solvents: solvent-inputs: solvent-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null FROMP Measurements: Measured frontal velocity (mm/s): 0.1821 Measured frontal velocity with light exposure (mm/s): null Measured maximum temperature (°C): null Type of front: SPIN	Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Nov 15, 2024

Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Nov 15, 2024

Batch ID: 30-10-2024 15:30 ACC
procedure:
- general:
  - Operator Initials: ACC
  - Mix Date and Time: 2024-10-30 15:30:00
  - Polymerization Date and Time: 2024-10-30 00:00:00
  - Resin Storage Temperature (°C): null
  - Resin Storage atmosphere: null
  - Resin Storage location: null
  - Polymer Storage Temperature (°C): null
  - Polymer Storage armosphere: null
  - Polymer Storage location: null
  - Mixing Conditions: null
  - Mixing Type: Sonication
  - Mixing Time (min): 2
  - Preparation temperature (°C): 19
  - Use Glovebox: NO
  - Polymerization: null
  - Type of polymerization: FROMP
  - Ambient temperature (°C): 21
  - Resin temperaure at the start of polymerization (°C): 23.1
  - Select Geometry from geometries tab: null
  - Geometry - Select from library: TUBE-2
  - Resin height (mm): 65
  - Diameter (mm): 9.74
  - Thickness (mm): 0.31
  - Tube length (mm): 75
  - Empty-dim: null
  - Initiation: null
  - Initiation method: THERMAL
  - Photocontrol: null
  - Photocontrol?: NO
  - null: null
- thermal initiation:
  - Heat Source: RESISTIVE WIRE
  - Heat Source Name: Kanthal A-1 Annealed ROUND Resistance Wire 24GA
  - Heater diameter (mm): 0.5105
  - Submerged length (mm): null
  - Power (W): null
  - Voltage (V): 4
  - Current (A): 4
  - Heat source temperature (°C): null
  - Induction time (s): until front starts
inputs:
- monomers:
  - monomer-inputs:
    - - name: COD
      - SMILES: C1/C=C\CC/C=C\C1
      - Measured mass (g): 1.9392744211349495
      - Measured volume (μL): null
      - Computed mass (g): 1.9392744211349495
      - Molecular Weight: 108.18
      - Moles: 1.79e-02
      - Monomer mol%: 97.26
    - - name: ENB
      - SMILES: CC=C1CC2CC1C=C2
      - Measured mass (g): 0.06072557886505048
      - Measured volume (μL): null
      - Computed mass (g): 0.06072557886505048
      - Molecular Weight: 120.2
      - Moles: 5.05e-04
      - Monomer mol%: 2.74
  - monomer-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): 20
    - Mixing type: N/A
    - Mixing time (mins): null
- catalysts:
  - catalyst-inputs:
    - - name: GC2, M204
      - SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
      - Measured mass (mg): 15.62
      - Computed mass (g): 0.015619999999999998
      - Molecular Weight: 848.98
      - Moles: 1.84e-05
      - Monomer:Catalyst molar ratio: 1001.79
  - catalyst-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): 21
    - Mixing type: Sonication
    - Mixing time (mins): 2
- inhibitors:
  - inhibitor-inputs:
    - - name: Tributyl phosphite (TBP)
      - SMILES: CCCCOP(=O)(OCCCC)OCCCC
      - Measured volume (μL): 10
      - Density: 0.925
      - Computed mass (mg): 0.009250000000000001
      - Molecular Weight: 250.3
      - Moles: 3.70e-05
      - Inhibitor:Catalyst molar ratio: 2.01
  - inhibitor-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
- additives:
  - additive-inputs:
  - additive-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
- solvents:
  - solvent-inputs:
  - solvent-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
FROMP Measurements:
- Measured frontal velocity (mm/s): 0.1821
- Measured frontal velocity with light exposure (mm/s): null
- Measured maximum temperature (°C): null
- Type of front: SPIN

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AC-1-252_COD/ENB_1000-1-2-A

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