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  2. AC-1-252_COD/E...

AC-1-252_COD/ENB_40000-1-2-A

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Description:

Monomer:G2:TBP 40000:1:2. 97/3 vol% COD/ENB measured by mass from a large batch. FROMPed at initial resin temperature of 23 degrees C.

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Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 30-10-2024 16:15 ACC
  • procedure:
    • general:
      • Operator Initials: ACC
      • Mix Date and Time: 2024-10-30 16:15:00
      • Polymerization Date and Time: 2024-10-30 00:00:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 2
      • Preparation temperature (°C): 19
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): 21
      • Resin temperaure at the start of polymerization (°C): 22.8
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-2
      • Resin height (mm): 65
      • Diameter (mm): 9.74
      • Thickness (mm): 0.31
      • Tube length (mm): 75
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: RESISTIVE WIRE
      • Heat Source Name: Kanthal A-1 Annealed ROUND Resistance Wire 24GA
      • Heater diameter (mm): 0.5105
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): 5
      • Current (A): 5
      • Heat source temperature (°C): null
      • Induction time (s): until front starts
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: COD
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 5.817823263404849
          • Measured volume (μL): null
          • Computed mass (g): 5.817823263404849
          • Molecular Weight: 108.18
          • Moles: 5.38e-02
          • Monomer mol%: 97.26
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.18217673659515143
          • Measured volume (μL): null
          • Computed mass (g): 0.18217673659515143
          • Molecular Weight: 120.2
          • Moles: 1.52e-03
          • Monomer mol%: 2.74
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 20
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC2, M204
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 1.17
          • Computed mass (g): 0.00117
          • Molecular Weight: 848.98
          • Moles: 1.38e-06
          • Monomer:Catalyst molar ratio: 40123.17
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 21
        • Mixing type: Sonication
        • Mixing time (mins): 2
    • inhibitors:
      • inhibitor-inputs:
          • name: Tributyl phosphite (TBP)
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.74
          • Density: 0.925
          • Computed mass (mg): 0.0006845
          • Molecular Weight: 250.3
          • Moles: 2.73e-06
          • Inhibitor:Catalyst molar ratio: 1.98
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.1014
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: SPIN
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Nov 15, 2024
  • Batch ID: 30-10-2024 16:15 ACC
  • procedure:
    • general:
      • Operator Initials: ACC
      • Mix Date and Time: 2024-10-30 16:15:00
      • Polymerization Date and Time: 2024-10-30 00:00:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 2
      • Preparation temperature (°C): 19
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): 21
      • Resin temperaure at the start of polymerization (°C): 22.8
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-2
      • Resin height (mm): 65
      • Diameter (mm): 9.74
      • Thickness (mm): 0.31
      • Tube length (mm): 75
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: RESISTIVE WIRE
      • Heat Source Name: Kanthal A-1 Annealed ROUND Resistance Wire 24GA
      • Heater diameter (mm): 0.5105
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): 5
      • Current (A): 5
      • Heat source temperature (°C): null
      • Induction time (s): until front starts
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: COD
          • SMILES: C1/C=C\CC/C=C\C1
          • Measured mass (g): 5.817823263404849
          • Measured volume (μL): null
          • Computed mass (g): 5.817823263404849
          • Molecular Weight: 108.18
          • Moles: 5.38e-02
          • Monomer mol%: 97.26
          • name: ENB
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.18217673659515143
          • Measured volume (μL): null
          • Computed mass (g): 0.18217673659515143
          • Molecular Weight: 120.2
          • Moles: 1.52e-03
          • Monomer mol%: 2.74
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 20
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC2, M204
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 1.17
          • Computed mass (g): 0.00117
          • Molecular Weight: 848.98
          • Moles: 1.38e-06
          • Monomer:Catalyst molar ratio: 40123.17
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): 21
        • Mixing type: Sonication
        • Mixing time (mins): 2
    • inhibitors:
      • inhibitor-inputs:
          • name: Tributyl phosphite (TBP)
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.74
          • Density: 0.925
          • Computed mass (mg): 0.0006845
          • Molecular Weight: 250.3
          • Moles: 2.73e-06
          • Inhibitor:Catalyst molar ratio: 1.98
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.1014
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: SPIN
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Fri Nov 15 03:34:29 UTC 2024 PROCESS: Uploading dataset metadata.

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Last viewed: Nov 28, 2024 22:38:21
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Last downloaded: Never
Last Modified: Nov 15, 2024 15:44:43

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