Clowder
  1. DSC Cure Kinetics
  2. 2023-10-28 CH D...

2023-10-28 CH DCPD TBP_GC2 CH10-28_unsizedprepreg_4 hr

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Description:

Prepreg dataset 12K AS4 CF, unsized

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Metadata

Name Value Last Modified
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: CH10-28_unsizedprepreg_4 hr
    • Sample Mass (mg): 13.230 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 2023-10-28 23:15:50
    • Operator: CH
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 87.456
    • Peak temperature (°C): 57.47
    • Onset x (°C): 48.397
    • Max Heat Flow: 10.64
    • Min Baseline Temp: 30.0
    • Max Baseline Temp: 85.0
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jan 9, 2025
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: CH10-28_unsizedprepreg_4 hr
    • Sample Mass (mg): 13.230 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 2023-10-28 23:15:50
    • Operator: CH
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 87.456
    • Peak temperature (°C): 57.47
    • Onset x (°C): 48.397
    • Max Heat Flow: 10.64
    • Min Baseline Temp: 30.0
    • Max Baseline Temp: 85.0
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jan 9, 2025
Batch ID
  • Batch ID: 28-10-2023 18:10 CH
  • procedure:
    • general:
      • Operator Initials: CH
      • Mix Date and Time: 2023-10-28 18:10:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: null
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: null
      • Photocontrol: null
      • Photocontrol?: null
      • null: null
    • photo control:
      • In situ light : null
      • Light wavelength (nm): null
      • Light Intensity (W/mm^2): null
      • Exposure duration (s): null
      • Exposure area (mm^2): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 5.9185
          • Measured volume (μL): null
          • Computed mass (g): 5.9185
          • Molecular Weight: 132.2
          • Moles: 4.48e-02
          • Monomer mol%: 94.53
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.3115
          • Measured volume (μL): null
          • Computed mass (g): 0.3115
          • Molecular Weight: 120.2
          • Moles: 2.59e-03
          • Monomer mol%: 5.47
      • monomer-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: Grubbs Catalyst gen-2 (GC2 - M204)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 4.02
          • Computed mass (g): 0.004019999999999999
          • Molecular Weight: 848.98
          • Moles: 4.74e-06
          • Monomer:Catalyst molar ratio: 10002.08
      • catalyst-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: Tributyl Phosphite (TBP)
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 1.28
          • Density: 0.925
          • Computed mass (mg): 0.0011840000000000002
          • Molecular Weight: 250.3
          • Moles: 4.73e-06
          • Inhibitor:Catalyst molar ratio: 1.0
      • inhibitor-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jan 9, 2025
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: CH10-28_unsizedprepreg_4 hr
    • Sample Mass (mg): 13.230 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 2023-10-28 23:15:50
    • Operator: CH
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 87.456
    • Peak temperature (°C): 57.47
    • Onset x (°C): 48.397
    • Max Heat Flow: 10.64
    • Min Baseline Temp: 30.0
    • Max Baseline Temp: 85.0
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: CH10-28_unsizedprepreg_4 hr
    • Sample Mass (mg): 13.230 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 2023-10-28 23:15:50
    • Operator: CH
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 87.456
    • Peak temperature (°C): 57.47
    • Onset x (°C): 48.397
    • Max Heat Flow: 10.64
    • Min Baseline Temp: 30.0
    • Max Baseline Temp: 85.0
  • Batch ID: 28-10-2023 18:10 CH
  • procedure:
    • general:
      • Operator Initials: CH
      • Mix Date and Time: 2023-10-28 18:10:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: null
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: null
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: null
      • Photocontrol: null
      • Photocontrol?: null
      • null: null
    • photo control:
      • In situ light : null
      • Light wavelength (nm): null
      • Light Intensity (W/mm^2): null
      • Exposure duration (s): null
      • Exposure area (mm^2): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 5.9185
          • Measured volume (μL): null
          • Computed mass (g): 5.9185
          • Molecular Weight: 132.2
          • Moles: 4.48e-02
          • Monomer mol%: 94.53
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.3115
          • Measured volume (μL): null
          • Computed mass (g): 0.3115
          • Molecular Weight: 120.2
          • Moles: 2.59e-03
          • Monomer mol%: 5.47
      • monomer-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: Grubbs Catalyst gen-2 (GC2 - M204)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 4.02
          • Computed mass (g): 0.004019999999999999
          • Molecular Weight: 848.98
          • Moles: 4.74e-06
          • Monomer:Catalyst molar ratio: 10002.08
      • catalyst-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: Tributyl Phosphite (TBP)
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 1.28
          • Density: 0.925
          • Computed mass (mg): 0.0011840000000000002
          • Molecular Weight: 250.3
          • Moles: 4.73e-06
          • Inhibitor:Catalyst molar ratio: 1.0
      • inhibitor-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: null
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
Extractor Started Latest Update Latest Status
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Timestamp Status Message
Thu Jan 09 16:00:01 UTC 2025 PROCESS: Uploading dataset metadata.
Timestamp Status Message
Thu Jan 09 15:59:42 UTC 2025 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Thu Jan 09 15:59:40 UTC 2025 PROCESS: Uploading dataset metadata.

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Last viewed: May 20, 2025 21:01:45
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Last downloaded: Never
Last Modified: Apr 29, 2025 15:43:09

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