| Batch ID |
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Batch ID:
10-1-2023 10:00 AC
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procedure:
-
general:
-
Operator Initials:
AC
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Mix Date and Time:
2023-01-10 10:00:00
-
Polymerization Date and Time:
2023-01-10 10:00:00
-
Resin Storage Temperature (°C):
null
-
Resin Storage atmosphere:
null
-
Resin Storage location:
null
-
Polymer Storage Temperature (°C):
null
-
Polymer Storage armosphere:
null
-
Polymer Storage location:
null
-
Mixing Conditions:
null
-
Mixing Type:
Sonication
-
Mixing Time (min):
2
-
Preparation temperature (°C):
21
-
Use Glovebox:
NO
-
Polymerization:
null
-
Type of polymerization:
FROMP
-
Ambient temperature (°C):
21
-
Resin temperaure at the start of polymerization (°C):
null
-
Select Geometry from geometries tab:
null
-
Geometry - Select from library:
TUBE-3
-
Resin height (mm):
32
-
Diameter (mm):
9.74
-
Thickness (mm):
0.52
-
Tube length (mm):
77.96
-
Post Cure Sampling Location:
Bulk
-
Empty-dim:
null
-
Initiation:
null
-
Initiation method:
CHEMICAL
-
Photocontrol:
null
-
Photocontrol?:
NO
-
null:
null
-
chemical initiation:
-
initiator-catalyst-solvent-concentration-mg/microL:
33.333333333333336
-
initiator-catalyst-solvent-concentration-moles/L:
4.586629973626878E-9
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initiator-inputs:
-
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name:
GC-3 (Grubbs Catalyst gen-3 H-substituted)
-
SMILES:
Cl[Ru](=C1N(C2=C(C)C=C(C)C=C2C)CCN1C3=C(C)C=C(C)C=C3C)([N]4=CC=CC=C4)(Cl)([N]5=CC=CC=C5)=CC6=CC=CC=C6
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Role:
Catalyst
-
Measured mass (mg):
2
-
Measured volume (μL):
null
-
Molecular Weight:
726.75
-
Moles:
2.75e-03
-
-
name:
toluene
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SMILES:
CC1=CC=CC=C1
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Role:
Solvent
-
Measured mass (mg):
null
-
Measured volume (μL):
60
-
Molecular Weight:
92.14
-
Moles:
5.65e-04
-
initiator-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
RT
-
Mixing type:
Sonication
-
Mixing time (mins):
1
-
Total volume used for initiation (μL):
20
-
inputs:
-
monomers:
-
monomer-inputs:
-
-
name:
Ethylidene Norbornene (ENB)
-
SMILES:
CC=C1CC2CC1C=C2
-
Measured mass (g):
0.37
-
Measured volume (μL):
null
-
Computed mass (g):
0.37
-
Molecular Weight:
120.2
-
Moles:
3.08e-03
-
Monomer mol%:
5.17
-
-
name:
Dicyclopentadiene (DCPD)
-
SMILES:
C1C=CC2C1C3CC2C=C3
-
Measured mass (g):
7.47
-
Measured volume (μL):
null
-
Computed mass (g):
7.47
-
Molecular Weight:
132.2
-
Moles:
5.65e-02
-
Monomer mol%:
94.83
-
monomer-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
RT
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
catalysts:
-
catalyst-inputs:
-
-
name:
GC-2
-
SMILES:
CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
-
Measured mass (mg):
6.28
-
Computed mass (g):
0.00628
-
Molecular Weight:
848.98
-
Moles:
7.40e-06
-
Monomer:Catalyst molar ratio:
8054.97
-
catalyst-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
RT
-
Mixing type:
Sonication
-
Mixing time (mins):
3
-
inhibitors:
-
inhibitor-inputs:
-
-
name:
TBP
-
SMILES:
CCCCOP(=O)(OCCCC)OCCCC
-
Measured volume (μL):
2
-
Density:
0.925
-
Computed mass (mg):
0.00185
-
Molecular Weight:
250.3
-
Moles:
7.39e-06
-
Inhibitor:Catalyst molar ratio:
1.0
-
inhibitor-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
additives:
-
additive-inputs:
-
additive-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
solvents:
-
solvent-inputs:
-
solvent-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
FROMP Measurements:
-
Measured frontal velocity (mm/s):
1.32
-
Measured frontal velocity with light exposure (mm/s):
null
-
Measured maximum temperature (°C):
244.421
-
Type of front:
LINEAR
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Extracted by
https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel
on Apr 25, 2025
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