| Batch ID |
-
Batch ID:
13-6-2023 08:00 LDM
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procedure:
-
general:
-
Operator Initials:
LDM
-
Mix Date and Time:
06/13/2023 8:00
-
Polymerization Date and Time:
06/13/2023 8:05
-
Resin Storage Temperature (°C):
20
-
Resin Storage atmosphere:
50
-
Resin Storage location:
Oven
-
Polymer Storage Temperature (°C):
null
-
Polymer Storage armosphere:
null
-
Polymer Storage location:
null
-
Mixing Conditions:
null
-
Mixing Type:
Sonication
-
Mixing Time (min):
5
-
Preparation temperature (°C):
25
-
Use Glovebox:
NO
-
Polymerization:
null
-
Type of polymerization:
NONE
-
Ambient temperature (°C):
null
-
Resin temperaure at the start of polymerization (°C):
null
-
Select Geometry from geometries tab:
null
-
Geometry - Select from library:
TUBE-1
-
Resin height (mm):
1
-
Diameter (mm):
2
-
Thickness (mm):
3
-
Tube length (mm):
1
-
Empty-dim:
null
-
Initiation:
null
-
Initiation method:
THERMAL
-
Photocontrol:
null
-
Photocontrol?:
NO
-
null:
null
-
thermal initiation:
-
Heat Source:
SOLDERING IRON
-
Heat Source Name:
null
-
Heater diameter (mm):
30
-
Submerged length (mm):
null
-
Power (W):
2
-
Voltage (V):
1
-
Current (A):
2
-
Heat source temperature (°C):
null
-
Induction time (s):
null
-
inputs:
-
monomers:
-
monomer-inputs:
-
-
name:
5-Norbornen-2-yl acetate
-
SMILES:
CC(=O)OC1CC2CC1C=C2
-
Measured mass (g):
1.908
-
Measured volume (μL):
null
-
Computed mass (g):
1.908
-
Molecular Weight (g/mol):
152.19
-
Moles:
1.25e-02
-
Monomer mol%:
94.25
-
-
name:
Ethylidene Norbornene (ENB)
-
SMILES:
CC=C1CC2CC1C=C2
-
Measured mass (g):
0.092
-
Measured volume (μL):
null
-
Computed mass (g):
0.092
-
Molecular Weight (g/mol):
120.2
-
Moles:
7.65e-04
-
Monomer mol%:
5.75
-
monomer-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
catalysts:
-
catalyst-inputs:
-
-
name:
Grubbs Catalyst gen-2 (GC2 - M202)
-
SMILES:
[Cl-][Ru+6]([Cl-])(=[C-2]1C=C(C=2C=CC=CC2)C=3C=CC=CC31)(=[C-2]4N(C=5C(=CC(=CC5C)C)C)CCN4C=6C(=CC(=CC6C)C)C)[P](C7CCCCC7)(C8CCCCC8)C9CCCCC9
-
Measured mass (mg):
5.16
-
Computed mass (g):
0.0051600000000000005
-
Molecular Weight (g/mol):
949.09
-
Moles:
5.44e-06
-
Monomer:Catalyst molar ratio:
2446.73
-
catalyst-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
Sonication
-
Mixing time (mins):
null
-
inhibitors:
-
inhibitor-inputs:
-
-
name:
Tributyl Phosphite (TBP)
-
SMILES:
CCCCOP(=O)(OCCCC)OCCCC
-
Measured volume (μL):
13.2
-
Density:
0.925
-
Computed mass (g):
0.01221
-
Molecular Weight (g/mol):
250.3
-
Moles:
4.88e-05
-
Inhibitor:Catalyst molar ratio:
8.97
-
inhibitor-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
additives:
-
additive-inputs:
-
-
name:
Fumed Silica (A200)
-
SMILES:
O=[Si]=O
-
Measured mass (g):
100
-
Measured volume (μL):
null
-
Computed mass (g):
100
-
Molecular Weight (g/mol):
60.08
-
Moles:
1.66e+00
-
Wt Percent of Additives:
98.03
-
additive-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
-
solvents:
-
solvent-inputs:
-
solvent-procedure:
-
Prepared in GloveBox?:
NO
-
Preparation temperature (°C):
null
-
Mixing type:
N/A
-
Mixing time (mins):
null
|
Extracted by
https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.batch.experiment.from_excel
on May 7, 2025
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