rhb_pag

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Description:

Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 10-3-2025 09:20 RHB
  • procedure:
    • general:
      • Operator Initials: RHB
      • Mix Date and Time: 2025-03-10 09:20:16
      • Polymerization Date and Time: 2025-03-10 09:20:16
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: SNL-1
      • Channel Length (mm): 36.57
      • Channel Width (mm): 9.74
      • Channel thickness (mm): 0.52
      • Photo Window y-location (mm): 77.96
      • Photo Window y-dimension (mm): null
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: YES
      • null: null
    • thermal initiation:
      • Heat Source: SOLDERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
    • photo control:
      • In situ light : YES
      • Preirradiation: NO
      • Light wavelength (nm): 385
      • Light Intensity (mW/cm^2): 30
      • Exposure duration (s): null
      • Exposure area (mm^2): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.3
          • Measured volume (μL): null
          • Computed mass (g): 0.3
          • Molecular Weight (g/mol): 120.2
          • Moles: 2.50e-03
          • Monomer mol%: 4.2
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 5.7
          • Measured volume (μL): null
          • Computed mass (g): 5.7
          • Molecular Weight (g/mol): 132.2
          • Moles: 4.31e-02
          • Monomer mol%: 72.48
          • name: OBNBD
          • SMILES: CC1(O2)C=CC2C3=C1C=CC=C3
          • Measured mass (g): 2
          • Measured volume (μL): null
          • Computed mass (g): 2
          • Molecular Weight (g/mol): 144.173
          • Moles: 1.39e-02
          • Monomer mol%: 23.32
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 24
          • Computed mass (g): 0.024
          • Molecular Weight (g/mol): 848.98
          • Moles: 2.83e-05
          • Monomer:Catalyst molar ratio: 2104.22
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): null
          • Density: 0.925
          • Computed mass (g): 0.0037
          • Molecular Weight (g/mol): 250.3
          • Moles: 1.48e-05
          • Inhibitor:Catalyst molar ratio: 0.52
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Anthracene
          • SMILES: C12=CC=CC=C1C=C3C=CC=CC3=C2
          • Measured mass (g): 0.02
          • Measured volume (μL): null
          • Computed mass (g): 0.02
          • Molecular Weight (g/mol): 178.23
          • Moles: 1.12e-04
          • Wt Percent of Additives: 0.25
          • name: N-hydroxynaphthalimide triflate
          • SMILES: O=C1N(C(C2=CC=CC3=CC=CC1=C23)=O)OS(=O)(C(F)(F)F)=O
          • Measured mass (g): 0.02
          • Measured volume (μL): null
          • Computed mass (g): 0.02
          • Molecular Weight (g/mol): 345.25
          • Moles: 5.79e-05
          • Wt Percent of Additives: 0.25
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): null
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on May 9, 2025
  • Batch ID: 10-3-2025 09:20 RHB
  • procedure:
    • general:
      • Operator Initials: RHB
      • Mix Date and Time: 2025-03-10 09:20:16
      • Polymerization Date and Time: 2025-03-10 09:20:16
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: SNL-1
      • Channel Length (mm): 36.57
      • Channel Width (mm): 9.74
      • Channel thickness (mm): 0.52
      • Photo Window y-location (mm): 77.96
      • Photo Window y-dimension (mm): null
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: YES
      • null: null
    • thermal initiation:
      • Heat Source: SOLDERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
    • photo control:
      • In situ light : YES
      • Preirradiation: NO
      • Light wavelength (nm): 385
      • Light Intensity (mW/cm^2): 30
      • Exposure duration (s): null
      • Exposure area (mm^2): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.3
          • Measured volume (μL): null
          • Computed mass (g): 0.3
          • Molecular Weight (g/mol): 120.2
          • Moles: 2.50e-03
          • Monomer mol%: 4.2
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 5.7
          • Measured volume (μL): null
          • Computed mass (g): 5.7
          • Molecular Weight (g/mol): 132.2
          • Moles: 4.31e-02
          • Monomer mol%: 72.48
          • name: OBNBD
          • SMILES: CC1(O2)C=CC2C3=C1C=CC=C3
          • Measured mass (g): 2
          • Measured volume (μL): null
          • Computed mass (g): 2
          • Molecular Weight (g/mol): 144.173
          • Moles: 1.39e-02
          • Monomer mol%: 23.32
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 24
          • Computed mass (g): 0.024
          • Molecular Weight (g/mol): 848.98
          • Moles: 2.83e-05
          • Monomer:Catalyst molar ratio: 2104.22
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): null
          • Density: 0.925
          • Computed mass (g): 0.0037
          • Molecular Weight (g/mol): 250.3
          • Moles: 1.48e-05
          • Inhibitor:Catalyst molar ratio: 0.52
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Anthracene
          • SMILES: C12=CC=CC=C1C=C3C=CC=CC3=C2
          • Measured mass (g): 0.02
          • Measured volume (μL): null
          • Computed mass (g): 0.02
          • Molecular Weight (g/mol): 178.23
          • Moles: 1.12e-04
          • Wt Percent of Additives: 0.25
          • name: N-hydroxynaphthalimide triflate
          • SMILES: O=C1N(C(C2=CC=CC3=CC=CC1=C23)=O)OS(=O)(C(F)(F)F)=O
          • Measured mass (g): 0.02
          • Measured volume (μL): null
          • Computed mass (g): 0.02
          • Molecular Weight (g/mol): 345.25
          • Moles: 5.79e-05
          • Wt Percent of Additives: 0.25
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): null
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Fri May 09 17:42:16 UTC 2025 PROCESS: Uploading dataset metadata.

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Last Modified: May 09, 2025 17:42:22

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