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  1. DSC Post Cures
  2. IA_10000_1_1

IA_10000_1_1

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Description:

This was an example we used during training

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Metadata

Name Value Last Modified
procedure
  • procedure:
    • Experiment Type: Custom
    • Sample Name: DCPD_ENB_GC2_TBP_10000_1_1_Modulated
    • Sample Mass (mg): 11.050 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 5/28/2025 9:14:35 AM
    • Operator: IA
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.2.101
    • Ramp rate (°C/min): 2.0
    • Ramp Min Temp (°C): 20.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Max Heat Flow: 0.75
    • Min Baseline Temp: 138.531
    • Max Baseline Temp: 181.211
    • Glass transition temperature: 157.371
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jun 12, 2025
Batch ID
  • Batch ID: 12-6-2025 14:49 IA
  • procedure:
    • general:
      • Operator Initials: IA
      • Mix Date and Time: 2025-06-12 14:49:00
      • Polymerization Date and Time: 2025-06-12 15:49:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): 20
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-1
      • Resin height (mm): 36.57
      • Diameter (mm): 9.74
      • Thickness (mm): 0.52
      • Tube length (mm): 77.96
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: SOLDERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.1
          • Measured volume (μL): null
          • Computed mass (g): 0.1
          • Molecular Weight (g/mol): 120.2
          • Moles: 8.32e-04
          • Monomer mol%: 5.47
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 1.9
          • Measured volume (μL): null
          • Computed mass (g): 1.9
          • Molecular Weight (g/mol): 132.2
          • Moles: 1.44e-02
          • Monomer mol%: 94.53
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: Grubbs Catalyst gen-2 (GC2 - M204)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 1.29
          • Computed mass (g): 0.0012900000000000001
          • Molecular Weight (g/mol): 848.98
          • Moles: 1.52e-06
          • Monomer:Catalyst molar ratio: 10006.19
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.4
          • Density: 0.925
          • Computed mass (g): 0.00037000000000000005
          • Molecular Weight (g/mol): 250.3
          • Moles: 1.48e-06
          • Inhibitor:Catalyst molar ratio: 0.97
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.98
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jun 12, 2025
  • procedure:
    • Experiment Type: Custom
    • Sample Name: DCPD_ENB_GC2_TBP_10000_1_1_Modulated
    • Sample Mass (mg): 11.050 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 5/28/2025 9:14:35 AM
    • Operator: IA
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.2.101
    • Ramp rate (°C/min): 2.0
    • Ramp Min Temp (°C): 20.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Max Heat Flow: 0.75
    • Min Baseline Temp: 138.531
    • Max Baseline Temp: 181.211
    • Glass transition temperature: 157.371
  • Batch ID: 12-6-2025 14:49 IA
  • procedure:
    • general:
      • Operator Initials: IA
      • Mix Date and Time: 2025-06-12 14:49:00
      • Polymerization Date and Time: 2025-06-12 15:49:00
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): 20
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: TUBE-1
      • Resin height (mm): 36.57
      • Diameter (mm): 9.74
      • Thickness (mm): 0.52
      • Tube length (mm): 77.96
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: SOLDERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.1
          • Measured volume (μL): null
          • Computed mass (g): 0.1
          • Molecular Weight (g/mol): 120.2
          • Moles: 8.32e-04
          • Monomer mol%: 5.47
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 1.9
          • Measured volume (μL): null
          • Computed mass (g): 1.9
          • Molecular Weight (g/mol): 132.2
          • Moles: 1.44e-02
          • Monomer mol%: 94.53
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: Grubbs Catalyst gen-2 (GC2 - M204)
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 1.29
          • Computed mass (g): 0.0012900000000000001
          • Molecular Weight (g/mol): 848.98
          • Moles: 1.52e-06
          • Monomer:Catalyst molar ratio: 10006.19
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 0.4
          • Density: 0.925
          • Computed mass (g): 0.00037000000000000005
          • Molecular Weight (g/mol): 250.3
          • Moles: 1.48e-06
          • Inhibitor:Catalyst molar ratio: 0.97
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.98
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Thu Jun 12 20:07:59 UTC 2025 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Thu Jun 12 20:07:40 UTC 2025 PROCESS: Uploading dataset metadata.

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Last viewed: Jun 14, 2025 17:06:32
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Last Modified: Jun 12, 2025 20:07:58

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