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  1. DSC Cure Kinetics
  2. MLI141 DCPD ENB...

MLI141 DCPD ENB GC2(M204) 10mol% DHF 1hr

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Description:

incubated for 1 hour

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Metadata

Name Value Last Modified
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: MLI141_10mol_1
    • Sample Mass (mg): 1.960 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 6/4/2025 11:17:04 AM
    • Operator: ML
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.2.101
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 250.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 297.13
    • Peak temperature (°C): 57.32
    • Onset x (°C): 40.194
    • Max Heat Flow: 2.18
    • Min Baseline Temp: 18.805
    • Max Baseline Temp: 146.327
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jun 13, 2025
Batch ID
  • Batch ID: 03-6-2025 10:09 ML
  • procedure:
    • general:
      • Operator Initials: ML
      • Mix Date and Time: 2025-06-03 10:09:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): null
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.200615
          • Measured volume (μL): null
          • Computed mass (g): 0.200615
          • Molecular Weight (g/mol): 120.2
          • Moles: 1.67e-03
          • Monomer mol%: 4.94
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 3.811685
          • Measured volume (μL): null
          • Computed mass (g): 3.811685
          • Molecular Weight (g/mol): 132.2
          • Moles: 2.88e-02
          • Monomer mol%: 85.3
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.2313
          • Measured volume (μL): null
          • Computed mass (g): 0.2313
          • Molecular Weight (g/mol): 70.1
          • Moles: 3.30e-03
          • Monomer mol%: 9.76
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.00281
          • Computed mass (g): 0.00000281
          • Molecular Weight (g/mol): 848.98
          • Moles: 3.31e-09
          • Monomer:Catalyst molar ratio: 10212322.29
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Butylated hydroxytoluene (BHT)
          • SMILES: CC(C)(C)c1cc(C)cc(c1O)C(C)(C)C
          • Measured mass (g): 0.03318
          • Measured volume (μL): null
          • Computed mass (g): 0.03318
          • Molecular Weight (g/mol): 220.356
          • Moles: 1.51e-04
          • Wt Percent of Additives: 0.78
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jun 13, 2025
Batch ID
  • Batch ID: 03-6-2025 10:09 ML
  • procedure:
    • general:
      • Operator Initials: ML
      • Mix Date and Time: 2025-06-03T10:09:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): null
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.200615
          • Measured volume (μL): null
          • Computed mass (g): 0.200615
          • Molecular Weight (g/mol): 120.2
          • Moles: 1.67e-03
          • Monomer mol%: 4.94
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 3.811685
          • Measured volume (μL): null
          • Computed mass (g): 3.811685
          • Molecular Weight (g/mol): 132.2
          • Moles: 2.88e-02
          • Monomer mol%: 85.3
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.2313
          • Measured volume (μL): null
          • Computed mass (g): 0.2313
          • Molecular Weight (g/mol): 70.1
          • Moles: 3.30e-03
          • Monomer mol%: 9.76
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.00281
          • Computed mass (g): 0.00000281
          • Molecular Weight (g/mol): 848.98
          • Moles: 3.31e-09
          • Monomer:Catalyst molar ratio: 10212322.29
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Butylated hydroxytoluene (BHT)
          • SMILES: CC(C)(C)c1cc(C)cc(c1O)C(C)(C)C
          • Measured mass (g): 0.03318
          • Measured volume (μL): null
          • Computed mass (g): 0.03318
          • Molecular Weight (g/mol): 220.356
          • Moles: 1.51e-04
          • Wt Percent of Additives: 0.78
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.batch.experiment.from_excel on Jun 13, 2025
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: MLI141_10mol_1
    • Sample Mass (mg): 1.960 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 6/4/2025 11:17:04 AM
    • Operator: ML
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.2.101
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 250.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 297.13
    • Peak temperature (°C): 57.32
    • Onset x (°C): 40.194
    • Max Heat Flow: 2.18
    • Min Baseline Temp: 18.805
    • Max Baseline Temp: 146.327
  • Batch ID: 03-6-2025 10:09 ML
  • procedure:
    • general:
      • Operator Initials: ML
      • Mix Date and Time: 2025-06-03 10:09:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): null
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.200615
          • Measured volume (μL): null
          • Computed mass (g): 0.200615
          • Molecular Weight (g/mol): 120.2
          • Moles: 1.67e-03
          • Monomer mol%: 4.94
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 3.811685
          • Measured volume (μL): null
          • Computed mass (g): 3.811685
          • Molecular Weight (g/mol): 132.2
          • Moles: 2.88e-02
          • Monomer mol%: 85.3
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.2313
          • Measured volume (μL): null
          • Computed mass (g): 0.2313
          • Molecular Weight (g/mol): 70.1
          • Moles: 3.30e-03
          • Monomer mol%: 9.76
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.00281
          • Computed mass (g): 0.00000281
          • Molecular Weight (g/mol): 848.98
          • Moles: 3.31e-09
          • Monomer:Catalyst molar ratio: 10212322.29
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Butylated hydroxytoluene (BHT)
          • SMILES: CC(C)(C)c1cc(C)cc(c1O)C(C)(C)C
          • Measured mass (g): 0.03318
          • Measured volume (μL): null
          • Computed mass (g): 0.03318
          • Molecular Weight (g/mol): 220.356
          • Moles: 1.51e-04
          • Wt Percent of Additives: 0.78
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • Batch ID: 03-6-2025 10:09 ML
  • procedure:
    • general:
      • Operator Initials: ML
      • Mix Date and Time: 2025-06-03T10:09:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 5
      • Preparation temperature (°C): null
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.200615
          • Measured volume (μL): null
          • Computed mass (g): 0.200615
          • Molecular Weight (g/mol): 120.2
          • Moles: 1.67e-03
          • Monomer mol%: 4.94
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 3.811685
          • Measured volume (μL): null
          • Computed mass (g): 3.811685
          • Molecular Weight (g/mol): 132.2
          • Moles: 2.88e-02
          • Monomer mol%: 85.3
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.2313
          • Measured volume (μL): null
          • Computed mass (g): 0.2313
          • Molecular Weight (g/mol): 70.1
          • Moles: 3.30e-03
          • Monomer mol%: 9.76
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.00281
          • Computed mass (g): 0.00000281
          • Molecular Weight (g/mol): 848.98
          • Moles: 3.31e-09
          • Monomer:Catalyst molar ratio: 10212322.29
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Butylated hydroxytoluene (BHT)
          • SMILES: CC(C)(C)c1cc(C)cc(c1O)C(C)(C)C
          • Measured mass (g): 0.03318
          • Measured volume (μL): null
          • Computed mass (g): 0.03318
          • Molecular Weight (g/mol): 220.356
          • Moles: 1.51e-04
          • Wt Percent of Additives: 0.78
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extractor Started Latest Update Latest Status
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Timestamp Status Message
Fri Jun 13 18:17:29 UTC 2025 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Fri Jun 13 18:17:29 UTC 2025 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Fri Jun 13 18:17:29 UTC 2025 PROCESS: Uploading dataset metadata.

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Last Modified: Jun 13, 2025 18:17:29

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