5k_005_1

Owner: Brandon Clarke
Created on Nov 07, 2025

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Name	Value	Last Modified
Batch ID	Batch ID: 20-10-2024 20:43 IA procedure: general: Operator Initials: IA Mix Date and Time: 2024-10-20 20:43:00 Polymerization Date and Time: 2024-10-20 21:28:00 Resin Storage Temperature (°C): null Resin Storage atmosphere: null Resin Storage location: null Polymer Storage Temperature (°C): null Polymer Storage armosphere: null Polymer Storage location: null Mixing Conditions: null Mixing Type: Sonication Mixing Time (min): 5 Preparation temperature (°C): null Use Glovebox: NO Polymerization: null Type of polymerization: FROMP Ambient temperature (°C): 25 Resin temperaure at the start of polymerization (°C): null Select Geometry from geometries tab: null Geometry - Select from library: TUBE-1 Resin height (mm): 36.57 Diameter (mm): 9.74 Thickness (mm): 0.52 Tube length (mm): 77.96 Empty-dim: null Initiation: null Initiation method: THERMAL Photocontrol: null Photocontrol?: NO null: null thermal initiation: Heat Source: SOLDERING IRON Heat Source Name: null Heater diameter (mm): null Submerged length (mm): null Power (W): null Voltage (V): null Current (A): null Heat source temperature (°C): null Induction time (s): null inputs: monomers: monomer-inputs: name: Ethylidene Norbornene (ENB) SMILES: CC=C1CC2CC1C=C2 Measured mass (g): 0.26 Measured volume (μL): null Computed mass (g): 0.26 Molecular Weight (g/mol): 120.2 Moles: 2.16e-03 Monomer mol%: 4.99 name: Dicyclopentadiene (DCPD) SMILES: C1C=CC2C1C3CC2C=C3 Measured mass (g): 5.44 Measured volume (μL): null Computed mass (g): 5.44 Molecular Weight (g/mol): 132.2 Moles: 4.11e-02 Monomer mol%: 94.87 name: norbornene-functionalized PDMS (5kDa) SMILES: C1=CC2CCC1C2C(=O)OCCO[Si](C)(C){[<]O[Si](C)(C)[>]}70OCCCC Measured mass (g): 0.3 Measured volume (μL): null Computed mass (g): 0.3 Molecular Weight (g/mol): 5000.0 Moles: 6.00e-05 Monomer mol%: 0.14 monomer-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null catalysts: catalyst-inputs: name: GC-2 SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3 Measured mass (mg): 3.68 Computed mass (g): 0.00368 Molecular Weight (g/mol): 848.98 Moles: 4.33e-06 Monomer:Catalyst molar ratio: 10006.16 catalyst-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: Sonication Mixing time (mins): null inhibitors: inhibitor-inputs: name: TBP SMILES: CCCCOP(=O)(OCCCC)OCCCC Measured volume (μL): 1.2 Density: 0.925 Computed mass (g): 0.0011099999999999999 Molecular Weight (g/mol): 250.3 Moles: 4.43e-06 Inhibitor:Catalyst molar ratio: 1.02 inhibitor-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null additives: additive-inputs: additive-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null solvents: solvent-inputs: solvent-procedure: Prepared in GloveBox?: NO Preparation temperature (°C): null Mixing type: N/A Mixing time (mins): null FROMP Measurements: Measured frontal velocity (mm/s): 0.94 Measured frontal velocity with light exposure (mm/s): null Measured maximum temperature (°C): 240.5 Type of front: LINEAR	Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Nov 7, 2025

Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Nov 7, 2025

Batch ID: 20-10-2024 20:43 IA
procedure:
- general:
  - Operator Initials: IA
  - Mix Date and Time: 2024-10-20 20:43:00
  - Polymerization Date and Time: 2024-10-20 21:28:00
  - Resin Storage Temperature (°C): null
  - Resin Storage atmosphere: null
  - Resin Storage location: null
  - Polymer Storage Temperature (°C): null
  - Polymer Storage armosphere: null
  - Polymer Storage location: null
  - Mixing Conditions: null
  - Mixing Type: Sonication
  - Mixing Time (min): 5
  - Preparation temperature (°C): null
  - Use Glovebox: NO
  - Polymerization: null
  - Type of polymerization: FROMP
  - Ambient temperature (°C): 25
  - Resin temperaure at the start of polymerization (°C): null
  - Select Geometry from geometries tab: null
  - Geometry - Select from library: TUBE-1
  - Resin height (mm): 36.57
  - Diameter (mm): 9.74
  - Thickness (mm): 0.52
  - Tube length (mm): 77.96
  - Empty-dim: null
  - Initiation: null
  - Initiation method: THERMAL
  - Photocontrol: null
  - Photocontrol?: NO
  - null: null
- thermal initiation:
  - Heat Source: SOLDERING IRON
  - Heat Source Name: null
  - Heater diameter (mm): null
  - Submerged length (mm): null
  - Power (W): null
  - Voltage (V): null
  - Current (A): null
  - Heat source temperature (°C): null
  - Induction time (s): null
inputs:
- monomers:
  - monomer-inputs:
    - - name: Ethylidene Norbornene (ENB)
      - SMILES: CC=C1CC2CC1C=C2
      - Measured mass (g): 0.26
      - Measured volume (μL): null
      - Computed mass (g): 0.26
      - Molecular Weight (g/mol): 120.2
      - Moles: 2.16e-03
      - Monomer mol%: 4.99
    - - name: Dicyclopentadiene (DCPD)
      - SMILES: C1C=CC2C1C3CC2C=C3
      - Measured mass (g): 5.44
      - Measured volume (μL): null
      - Computed mass (g): 5.44
      - Molecular Weight (g/mol): 132.2
      - Moles: 4.11e-02
      - Monomer mol%: 94.87
    - - name: norbornene-functionalized PDMS (5kDa)
      - SMILES: C1=CC2CCC1C2C(=O)OCCO[Si](C)(C){[<]O[Si](C)(C)[>]}70OCCCC
      - Measured mass (g): 0.3
      - Measured volume (μL): null
      - Computed mass (g): 0.3
      - Molecular Weight (g/mol): 5000.0
      - Moles: 6.00e-05
      - Monomer mol%: 0.14
  - monomer-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
- catalysts:
  - catalyst-inputs:
    - - name: GC-2
      - SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
      - Measured mass (mg): 3.68
      - Computed mass (g): 0.00368
      - Molecular Weight (g/mol): 848.98
      - Moles: 4.33e-06
      - Monomer:Catalyst molar ratio: 10006.16
  - catalyst-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: Sonication
    - Mixing time (mins): null
- inhibitors:
  - inhibitor-inputs:
    - - name: TBP
      - SMILES: CCCCOP(=O)(OCCCC)OCCCC
      - Measured volume (μL): 1.2
      - Density: 0.925
      - Computed mass (g): 0.0011099999999999999
      - Molecular Weight (g/mol): 250.3
      - Moles: 4.43e-06
      - Inhibitor:Catalyst molar ratio: 1.02
  - inhibitor-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
- additives:
  - additive-inputs:
  - additive-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
- solvents:
  - solvent-inputs:
  - solvent-procedure:
    - Prepared in GloveBox?: NO
    - Preparation temperature (°C): null
    - Mixing type: N/A
    - Mixing time (mins): null
FROMP Measurements:
- Measured frontal velocity (mm/s): 0.94
- Measured frontal velocity with light exposure (mm/s): null
- Measured maximum temperature (°C): 240.5
- Type of front: LINEAR

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remat.experiment.from_excel

Fri Nov 07 20:20:58 UTC 2025

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Fri Nov 07 20:20:58 UTC 2025

PROCESS: Uploading dataset metadata.

Timestamp	Status Message
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5k_005_1

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