16af1227-4535-4eb2-9027-56a86e00a141

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Description:

Dataset created by CLI

Metadata

Name Value Last Modified
Batch ID
  • Batch ID: 20-6-2023 09:59 RM
  • procedure:
    • general:
      • Operator Initials: RM
      • Mix Date and Time: 2023-06-20 09:59:27
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: YES
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.033
          • Measured volume (μL): null
          • Computed mass (g): 0.033
          • Molecular Weight (g/mol): 120.2
          • Moles: 2.75e-04
          • Monomer mol%: 4.49
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 0.699
          • Measured volume (μL): null
          • Computed mass (g): 0.699
          • Molecular Weight (g/mol): 132.2
          • Moles: 5.29e-03
          • Monomer mol%: 86.38
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.0392
          • Measured volume (μL): null
          • Computed mass (g): 0.0392
          • Molecular Weight (g/mol): 70.1
          • Moles: 5.59e-04
          • Monomer mol%: 9.14
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.476
          • Computed mass (g): 0.00047599999999999997
          • Molecular Weight (g/mol): 848.98
          • Moles: 5.61e-07
          • Monomer:Catalyst molar ratio: 10917.57
      • catalyst-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: (11bS)-N,N-dimethyl-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-amine
          • SMILES: CN(C)P1Oc2ccc3CCCCc3c2-c4c(O1)ccc5CCCCc45
          • Measured volume (μL): null
          • Density: 1.0
          • Computed mass (g): 0.00019800000000000002
          • Molecular Weight (g/mol): 367.42
          • Moles: 5.39e-07
          • Inhibitor:Catalyst molar ratio: 0.96
      • inhibitor-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
          • name: Phenyl Cyclohexane
          • SMILES: C1CCC(=CC1)C2=CC=CC=C2
          • Measured mass (mg): null
          • Measured volume (μL): 17.5
          • Computed mass (g): 0.017185000000000002
          • Molecular Weight (g/mol): 160.26
          • Moles: 1.07e-04
          • Solvent concentration (mL/g): 36.76
      • solvent-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.experiment.from_excel on Jan 28, 2026
procedure
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: MonoPhos_cure_DHF-100_0
    • Sample Mass (mg): 11.270 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 6/20/2023 10:04:27 AM
    • Operator: Reid
    • Instrument Name: DSC2A-02712
    • Instrument Type: DSC250
    • Serial Number: DSC2A-02712
    • Location of Instrument: MFG
    • Trios version: 5.6.0.87
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 250.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 266.48
    • Peak temperature (°C): 121.13
    • Onset x (°C): 90.579
    • Max Heat Flow: 7.77
    • Min Baseline Temp: 24.216
    • Max Baseline Temp: 219.575
Extracted by https://re-mat.clowder.ncsa.illinois.edu/api/extractors/remat.parameters.from_txt on Jan 28, 2026
  • Batch ID: 20-6-2023 09:59 RM
  • procedure:
    • general:
      • Operator Initials: RM
      • Mix Date and Time: 2023-06-20 09:59:27
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): null
      • Preparation temperature (°C): null
      • Use Glovebox: YES
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: NONE
      • Empty-dim: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.033
          • Measured volume (μL): null
          • Computed mass (g): 0.033
          • Molecular Weight (g/mol): 120.2
          • Moles: 2.75e-04
          • Monomer mol%: 4.49
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 0.699
          • Measured volume (μL): null
          • Computed mass (g): 0.699
          • Molecular Weight (g/mol): 132.2
          • Moles: 5.29e-03
          • Monomer mol%: 86.38
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.0392
          • Measured volume (μL): null
          • Computed mass (g): 0.0392
          • Molecular Weight (g/mol): 70.1
          • Moles: 5.59e-04
          • Monomer mol%: 9.14
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.476
          • Computed mass (g): 0.00047599999999999997
          • Molecular Weight (g/mol): 848.98
          • Moles: 5.61e-07
          • Monomer:Catalyst molar ratio: 10917.57
      • catalyst-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: (11bS)-N,N-dimethyl-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-amine
          • SMILES: CN(C)P1Oc2ccc3CCCCc3c2-c4c(O1)ccc5CCCCc45
          • Measured volume (μL): null
          • Density: 1.0
          • Computed mass (g): 0.00019800000000000002
          • Molecular Weight (g/mol): 367.42
          • Moles: 5.39e-07
          • Inhibitor:Catalyst molar ratio: 0.96
      • inhibitor-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
      • additive-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
          • name: Phenyl Cyclohexane
          • SMILES: C1CCC(=CC1)C2=CC=CC=C2
          • Measured mass (mg): null
          • Measured volume (μL): 17.5
          • Computed mass (g): 0.017185000000000002
          • Molecular Weight (g/mol): 160.26
          • Moles: 1.07e-04
          • Solvent concentration (mL/g): 36.76
      • solvent-procedure:
        • Prepared in GloveBox?: YES
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: MonoPhos_cure_DHF-100_0
    • Sample Mass (mg): 11.270 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 6/20/2023 10:04:27 AM
    • Operator: Reid
    • Instrument Name: DSC2A-02712
    • Instrument Type: DSC250
    • Serial Number: DSC2A-02712
    • Location of Instrument: MFG
    • Trios version: 5.6.0.87
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 250.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 266.48
    • Peak temperature (°C): 121.13
    • Onset x (°C): 90.579
    • Max Heat Flow: 7.77
    • Min Baseline Temp: 24.216
    • Max Baseline Temp: 219.575
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Wed Jan 28 23:00:31 UTC 2026 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Wed Jan 28 22:50:13 UTC 2026 PROCESS: Uploading dataset metadata.

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Last viewed: Jan 29, 2026 07:23:15
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Last Modified: Jan 28, 2026 23:01:40

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